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The self-assembly of 1,3,4-thiadiazole-2,5-di-4-pyridyl (L 1 ), 4,4′-dipyridyl (L 2 ) with Zn(II), Cu(II) salts afforded one unusual coordination polymer with left-handed homo-chiral 3-D open MOFs in which supramolecular left-handed methanol helices were selectively formed, and one 2-D coordination polymer where two-fold interpenetrated 3-D supramolecular frameworks were constructed...
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