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A cobalt-organic framework (1) consisted of close-packed polyhedral cages is isostructural to CPM-35-Ni. The activated sample (1a) can adsorb high H2 uptake of 88.3cm3g−1 (0.79wt.%) at 77K and 1.0bar. Remarkably, 1a shows high CO2 adsorption capacity and good adsorption selectivity for CO2 over CH4 and N2.
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