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Direct template macrobicyclization of three 1,2-cyclohexanedione dioxime molecules with monofunctionalized HO-, H 2 N- and HOOC-containing phenylboronic acids on Fe 2+ and Co 2+ ions as a matrix afforded new macrobicyclic iron and cobalt(II) tris-dioximates with reactive apical substituents. The clathrochelates synthesized has been characterized by spectroscopic methods, X-ray...
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