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Ethanol electrooxidation reaction (EOR) pathways on polycrystalline platinum were studied with broadband sum-frequency generation (BB-SFG) spectroscopy and electrochemistry in unprecedented detail and under working fuel cell conditions. We present the first observation of adsorbed acetate and co-adsorbed sulfuric acid anions with SFG and a discussion of their relation to the EOR. Surface-adsorbed...
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