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We have previously reported the superior catalytic activity of Pd-NiO/SiO2 to Pd-Ni/SiO2 in hydrogenation of α-angelica lactone (α-AL) to gamma-valerolactone (GVL) in a batch reactor. To gain deeper insight into the structure-activity relationship of Pd-Ni bimetal catalyst, a series of NiO/SiO2 with different NiO particle sizes (about 3, 9, and 20nm in average) were prepared by impregnation method...
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