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The carbon-doped SiB ∼30 compound was obtained during attempts to synthesize by arc-melting boron-rich binaries belonging to the SiB n solid solution (13<n<32). Its crystal structure was determined from X-ray single-crystal intensity data (R-3m, Z=1, a=11.0152(3)Å, and c=23.8625(8)Å) and led to the final formula SiB ∼30 C 0.35 . Carbon is incorporated fortuitously...
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