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Melting reactions of Cu, CuCl, S, and Bi 2 S 3 yield black, shiny needles of Cu 22(1) Bi 12 S 21(1) Cl 16(1) . The compound decomposes peritectically at 649(5)K. Oxidation state +I of the copper atoms is supported by Cu–K-XANES. The compound crystallizes in the hexagonal space group P6/m with a=2116.7(7)pm and c=395.17(5)pm. Seven anions coordinate each...
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