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Oxides precursors ZrxTi1−xO2(x=0.22, 0.39, and 0.60) were prepared by a hydrolytic sol–gel process. The amorphous mixed oxides are homogeneous as deduced from electron microscopy and XPS studies. The crystallization of these amorphous oxides was studied by TGA–DTA and thermodiffractometry. Quantitative analysis of the crystalline phases, obtained at 1000°C, was carried out by the Rietveld method....
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