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An amylose-like α-(1,4)-glucan was synthesized by polycondensation and subsequent deprotection of a partially benzylated phenyl 1-thio-β-maltooctaoside having a sole hydroxyl group at the non-reducing end. The key octasaccharide monomer 6 was prepared by means of a single-site acetolytic reaction of fully acetylated γ-cyclodextrin and several subsequent chemical manipulations at its reducing and non-reducing...
Highly porous beads having an ability to form inclusion complexes with specific substrates have been synthesized and preliminary experiments for the application to adsorbent for affinity column chromatography and controlled release were carried out. Water-insoluble chitosan beads were synthesized by adding an aqueous acetic acid solution of chitosan into ethanolic aqueous sodium hydroxide and subsequent...
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