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The utility of combining chiral derivatization and solid-phase microextraction (SPME) for the enantiomeric analysis of primary amphetamines by liquid chromatography has been investigated. Different derivatization/extraction strategies have been evaluated and compared using the chiral reagent o-phthaldialdehyde (OPA)–N-acetyl-l-cysteine (NAC) and fibres with a Carbowax-templated resin coating. Amphetamine,...
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