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The complete 1 H and 13 C NMR assignments of a series of tertiary phosphonoacetamides (1) with different N-substitution patterns are reported. N,N-Dialkyl derivatives show two sets of signals due to hindered rotation of the (O)CN bond, which originate E/Z diastereoisomers for unsymmetrically N,N-disubstituted derivatives. Complete assignment of the 1 H NMR resonances of both...
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