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The molecular structure and conformational composition of tetrahydrofurfuryl alcohol in the gas-phase has been studied by a joint electron diffraction/ab initio method. The most abundant (84 ± 8%) conformer (A) in the gas-phase mixture was found to be stabilized by hydrogen bonding and had the O-H group placed over the furanose ring, which had a distorted 4 T 3 conformation. The...
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