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Hydrothermal self-assembly of orotic acid (C5H4N2O4OrH3) with metal salt Cu(Ac)2·H2O yielded a new OrH based hydrogen bonded coordination network of formula [Cu(OrH)(2NH3)(H2O)]·H2O (1) and [Cu(OrH) (2NH3)]2 (2). Single crystal X–ray study on 1 confirms that +2 charges on the metal ions (Cu2+) are balanced by OrH anion. N–H⋯O and O–H⋯O hydrogen bonding synthons are the only artifact for the resulting...
An ionic coordination complex of manganese(III), [Mn(HL)2(CH3OH)2][Mn(HL)2(N3)2] (where H2L = 1-(5-hydroxy-3-oxapentyliminomethyl)-3-ethoxyphenol), has been synthesized. Elemental analyses and spectroscopic techniques have been used to characterize the complex. The structure has been determined by the single crystal X-ray diffraction study. The complex consists of a complex cation, [Mn(HL)2(CH3OH)...
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