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The synthesis of gold nanoparticles with controllable particle sizes and densities on platinum substrates was first developed by sonoelectrochemical methods in this study. First, an Au substrate was cycled in a deoxygenated aqueous solution containing 0.1M HCl from −0.28 to +1.22V vs. Ag/AgCl at 500mV/s with different scans. The durations at the cathodic and anodic vertexes are 10 and 5s, respectively...
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