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Chemical shifts and coupling constants of completely assigned 1 H and 13 C NMR spectra at 500 MHz, as well as ROESY and HMBC connectivities were used to establish the structure of the pentasaccharide Galβ(1 → 4)GlcNAcβ(1 → 3)[GlcNAcβ(1 → 6)]Galβ(1 → 4)GlcNAc, synthesized by the action of the mid-chain β-(1 → 6)-d-N-acetylglucosaminyltransferase of rat serum from UDP-GlcNAc and...
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