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The dissociation of a crystalline complex of cyclomaltohexaose (α-cyclodextrin) and 1-methylcyclopropene has been studied in response to stepwise rising relative humidity at 50°C using a dynamic vapor sorption instrument. The dissociation of the inclusion complex was monitored with a proton transfer reaction mass spectrometer. The increase in relative humidity generally triggered the complex dissociation...
Supramolecuar aggregations 1 and 2 were prepared by complexing cyclomaltohexaose with two azodipyridine isomers: 4,4′-azodipyridine and 2,2′-azodipyridine, and their binding abilities and assembly behaviors were investigated comprehensively by X-ray crystallography, 2D NMR spectroscopy, and isothermal titration calorimetry. In solution, 1:1 host–guest complexation is generally assumed, whereas in...
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