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Ruthenium nitrosonaphthol complexes incorporating pendant pyridyl ligands of trans- and cis-[Ru{η 2 -N(O)C 10 H 6 O} 2 (CO)(NC 5 H 4 CHCHC 5 H 4 N)] (1a and 1b) and trans- and cis-[Ru{η 2 -OC 10 H 6 N(O)} 2 (CO)(NC 5 H 4 CHCHC 5 H 4 N)] (1c and 1d) were synthesized and used as building blocks in the construction of a supramolecular system. The molecular structures of 1b and the NMe 3 substitution complex cis-[Ru{η 2 -N(O)C 10 H 6 O} 2 (CO)(NMe 3 )] (2b) were established by X-ray diffraction analysis.