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Crystal structure of the low temperature form of LiMn 2 O 4 has been successfully determined by using single-crystal X-ray diffraction data at 130 K. It belongs to the orthorhombic system, space group Fddd with a=24.750(3) A, b=24.801(2) A, c=8.1903(9) A, and V=5027.4(9) A 3 . The structure, including anisotropic displacement parameters for each atom, was refined to the conventional...
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