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A new facile and efficient one-pot procedure for the synthesis of 3-phenyl-3-silatetrahydropyrans with an easily functionalized Si–Ph bond was developed. The method is based on the intramolecular cyclization of chloromethyl(3-hydroxypropyl)phenylsilanes using the n-Bu 4 NBr/i-Pr 2 NEt combination. As an example of functionalization, the synthesis of the first 3-silatetrahydropyran...
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