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The SF 5 -analog of the Umemoto salt was synthesized in just two steps by combining our recently reported SF 5 -biaryl synthesis, via Suzuki coupling with 4-(pentafluorosulfanyl)benzenediazonium tetrafluoroborate, with Magnier's one-pot synthesis of dibenzothiophenium salts employing CF 3 SO 2 Na and triflic anhydride. The trifluoromethylating power of this novel onium...
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