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The relationship between the crystal packing of powder samples and long-range 13C–13C homonuclear dipolar couplings is presented and illustrated for the case of uniformly 13C-enriched l-alanine and l-histidine·HCl·H2O. Dipolar coupling measurement is based on the partial reintroduction of dipolar interactions by spinning the sample slightly off-magic-angle, while the coupling of interest for a given...
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