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A nanocrystalline alloy of Fe 51 Co 20 Ni 14 Zr 6 B 9 , was produced by mechanical alloying. The main structural analysis was carried out via X-ray diffraction. The spectra were analyzed by Rietveld refinement using the MAUD program. The as-milled, 10, 20, 40 and 80h alloys consisted primarily of metastable bcc-Fe(Co,Ni) nanocrystals reaching around 8nm mean...
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