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In this work, we report a novel synthesis of nanoscale anatase TiO 2 with dominant highly active {111} facets by a simple one-step hydrothermal route with the assistance of NH 4 F and HF. In this progress, the exposed crystal facets of TiO 2 can been directly tuned by controlling the mole ratio of NH 4+ and F − . When the mole ratio of NH 4+ ...
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