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We found that various layered double hydroxides (LDHs) showed good activity for the photocatalytic conversion of CO2 in an aqueous solution. Isotope experiments using 13CO2 as a substrate clearly revealed that CO was generated as a main reduction product of CO2. Ni–Al LDH (Ni/Al=4) exhibited the largest amount of CO evolved among the various kinds of LDHs. Especially, Ni–Al LDHs fabricated from chlorides...
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