Samples of the Fe 60 Co 13 Pr 9 B 14 Ti 3 Zr 1 alloy were produced in the form of: (a) ribbons of various thicknesses t by melt-spinning, (b) 1mm diameter rods and (c) thin-walled tubes of outer diameter (o.d.) 3mm, both by suction-casting methods. The microstructure of the thick ribbon samples (with t>100μm) was shown to be a mixture of amorphous and nanocrystalline phases. Furthermore, the rod and tube samples were nanocrystalline in the as-cast state. Relatively high values of coercivity μ 0J H c of ∼0.98 and 1.56T were measured, respectively, for the tube and ribbon samples.