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Bi 3-2x Ca 2x Fe 5-x-y In y V x O 12 crystals with the size of 20x20x15mm 3 were grown by TSSG technique. The optimized conditions to grow the crystal were obtained. The quality of the crystal was checked by X-ray powder diffraction pattern of samples from different sections of the grown crystal. Absorption coefficient of the crystal in near infrared region was measured. The relationship between magnetic susceptibility -1 and temperature was given.