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The ternary isobaric diagram, (PbO 2 -Pb-MoO 3 ), system in air has been drawn to determine the suitable conditions for the preparation of PbMoO 4 . Starting with PbO 2 instead of PbO, it was possible to prepare PbMoO 4 and Pb 2 MoO 5 at 405 and 430°C, respectively, instead of 650 and 760°C.