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The adsorption and oxidation of thiocyanate (SCN−) on polycrystalline Au electrode surface in acidic electrolyte (10mM NaSCN/0.1M HClO4) have been investigated with broadband sum-frequency generation spectroscopy (BB-SFG). Potential-dependent behaviors of both the surface adsorbed species and the Au nonresonant (NR) electrode surface have been observed through BB-SFG band. A phase change of the S-bounded...
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