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The effects of oxygen pick-up and Al atoms on the formation and microstructure of freestanding SiC(Al) films by melt spinning of polyaluminocarbosilane (PACS) precursor were studied. PACS green films were cross-linked for 1h, 2h, 3h and 4h, pre-pyrolyzed at 900°C, respectively. They were continuously pyrolyzed at 1800°C to convert initial PACS into SiC(Al) ceramic films. Results reveal that the strict...
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