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The reactivity of the metalloligand [Pt 2 (μ-S) 2 (PPh 3 ) 4 ] towards a wide range of platinum(II) and palladium(II) chloride complex substrates [L 2 MCl 2 ] has been explored, using the technique of electrospray ionisation mass spectrometry to directly analyse reaction solutions. In the majority of cases, products are formed by addition of the ML ...
On the basis of hard soft acid base theory, two neutral heterometallic M2Pd3 supramolecular cages, [Al2Pd3(L)6Cl6] (1) and [Fe2Pd3(L)6Cl6] (2) (where HL is 1-(4-(1H-imidazol-1-yl)phenyl)butane-1,3-dione), have been constructed by using the tripodal M(L)3 as metalloligands in combination with PdCl2 or Pd(MeCN)2Cl2. The supramolecular cage can be described as a trigonal bipyramid with two M3+ ions occupying...
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