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[Pd(HQS) 2 ] (HQS=8-hydroxyquinoline-5-sulfonic acid) efficiently catalyses the Suzuki–Miyaura reactions of a broad scope of bromobenzenes in neat water. Moreover, the catalysts can be recycled up to four times without any significant decrease in activity.
The sterically hindered thiolate complexes [Pd(SR) 2 (TMEDA)] SR=SC 6 F 5 (2), SC 6 F 4 -4-H (3), SC 6 H 4 -2-SiPh 3 (4) were easily synthesized by metathetical reactions of the corresponding palladium chloro compound [Pd(Cl) 2 (TMEDA)] (1) and the lead salt of the corresponding thiol. The identity of the three species being unequivocally...
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