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Two gadonilium DOTAM complexes [Gd(DOTAM)H 2 O](CF 3 SO 3 ) 3 ·3H 2 O (1) and [Gd(DOTAM)H 2 O](CF 3 SO 3 ) 3 ·0.5H 2 O·CH 3 CN (2) have the structure of the M isomer, with coordination geometry around the Gd ion capped square antiprismatic (SA). They differ for the Gd–O water bond lengths of 2.396(6) and...
The syntheses and X-ray crystal structures of the Eu, Gd, Dy, Ho, and Er nitrate complexes of the pentadentate ligand 2,6-diacetylpyridine bis acetic acid hydrazone, or H 2 dapaah, are reported. The complexes can be divided into 3 groups depending on the number of water molecules per metal ion. The Ln·4H 2 O complexes with Eu, Gd and Dy are isomorphous, with the Ln ion being 10 coordinate...
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