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Styrenic polymers (XAD2 and XAD4) were hyper-cross-linked using dichloroalkane (-methane, -ethane, -butane, and -hexane) cross-linkers in the presence of a Friedel-Crafts catalyst (FeCl3). Hyper-cross-linking with dichloromethane generated the largest micropore volume increase; surface area and micropore volume decreased with increasing cross-linker length. Longer dichloroalkane cross-linkers also...
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