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CdS-PVP nanocomposites grown with various concentrations of Cd+/S− and PVP are studied using Raman and atomic force microscopy mapping on same selected areas. The study shows that CdS nanocrystals are embedded in either a thin-film or spheres of PVP, formation of which depends on relative ratio of Cd+/S− concentration (density of nanocrystals) to PVP. Collapse of PVP from planer matrix to the sphere...
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