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Soft-magnetic Fe 55 Co 45 alloy nanoparticles have been successfully synthesized by the polyol reduction process followed by annealing under argon. The diethylene glycol (DEG) was used as solvent and reducing agent simultaneously in this process. The synthesized samples of nanoparticles were annealed at 873K for different times. The alloy formation processes, the evolution of the microstructure,...
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