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A new diiron complex (μ-dmedt)[Fe2(CO)5IPr] (2, dmedt = 2,3-butanedithiol, IPr = 1,3-bis(2,6-diisopropylphenyl) imidazol-2-ylidene) was synthesized as analogue of the active site of [Fe-Fe]-H2ases. The sterically bulky nitrogen heterocyclic carbene ligand of IPr coordinated to the iron center was introduced via CO/L substitution reaction in mild conditions. The reactivity of electrocatalytic reduction...
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