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Nanocrystalline iron was obtained by reduction of magnetite doped with structural promoters at 773 K and characterized by various methods i.e. thermal desorption of gases (BET), X-ray diffraction (XRD) and inductively coupled plasma atomic emission spectroscopy (ICP-AES). Crystallite size distribution was determined using a novel method based on a phenomenon unique to nanomaterials, i.e. the dependence...
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