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The solid solution technique is one of the oldest but most powerful methods in the search for advanced materials. Hume-Rothery rules regarding solid solutions are well established for alloys, but little is known about oxides. In this study, we focused on the spinel oxides of Fe[Li1/2Fe3/2]O4−LiFeTiO4−Li[Li1/3Ti5/3]O4 to clarify their cation distribution, which necessitates other rules for substitutionally...
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