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This paper describes a microwell-based microdevice for performing quantitative bioanalysis. This microdevice combined the passive pumping by degassed polydimethylsiloxane (PDMS) with serial operations including solution dispensing, plates splitting and plates stacking. We name this microdevice “stacking chip”. To use the stacking chip in quantitative bioanalysis, nanoliter solutions were first dispensed...
Hydrogen peroxide (H2O2) is becoming significant due to its extensive applications, so determination of H2O2 is very important topic in analytical chemistry. Metal-free “graphene alloy” – nitrogen (N) and sulfur (S) heteroatoms co-doped reduced graphene oxide (NS-rGO) was produced via a simple one-step thermal annealing procedure using a mixture of 5-amino-2-mercapto-1,3,4-thiadiazole (AMT) and graphene...
A polymerized film of copper-2-amino-5-mercapto-1,3,4-thiadiazole (Cu(II)-AMT) complex (poly(Cu-AMT)) was successfully achieved via a simple and low-cost electrochemical methodology. Subsequently, a noncovalent nanohybrid of poly(Cu-AMT) with reduced graphene oxide (rGO) (rGO-poly(Cu-AMT)) was prepared through π–π stacking interaction as an efficient mimetic enzyme for the ultrasensitive and selective...
In this study, we proposed a method to fabricate magnetic carbon nitride (CN) nanosheets by simple physical blending. Low-cost CN nanosheets prepared by urea possessed a highly π-conjugated structure; therefore the obtained composites were employed as magnetic solid-phase extraction (MSPE) sorbent for extraction of polycyclic aromatic hydrocarbons (PAHs) in edible oil samples. Moreover, sample pre-treatment...
In this study, polyaniline coated SiO 2 nanofibers (PANI/SiO 2 ) was prepared by combining electrospinning technique with in-situ polymerization. The proposed strategy for the preparation of PANI/SiO 2 can eliminate the aggregation of PANI and the yield of PANI/SiO 2 was high. Scanning electron microscopy (SEM) images showed that PANI nanoparticles were uniformly coated...
In this study, a stir rod sorptive extraction (SRSE) adsorbent material was prepared by coating poly(4-vinylpyridine-co-ethylene glycol dimethacrylate) [poly(VP-co-EDMA)] monolithic polymer on stir rod, and then applied to the extraction of three non-steroidal anti-inflammatory drugs (NSAIDs) in environmental aqueous samples. The preparation conditions of monolithic material such as the amount of...
Simultaneous determination of tin, germanium and molybdenum in food samples has been established by flow injection-charge coupled detector (CCD) diode array detection spectrophotometry with partial least squares (PLS) algorithm. The method was based on the chromogenic reaction of metal ions and salicylflurone in the presence of cetyltrimethyl ammonium bromide. The overlapping spectra of these complexes...
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