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As opposed to the reversible redox reaction ({Fe(NO)2}10 reduced‐form DNIC [(NO)2Fe(S(CH2)3S)]2− (1)⇌{Fe(NO)2}9 oxidized‐form [(NO)2Fe(S(CH2)3S)]−), the chemical oxidation of the {Fe(NO)2}10 DNIC [(NO)2Fe(S(CH2)2S)]2− (2) generates the dinuclear {Fe(NO)2}9–{Fe(NO)2}9 complex [(NO)2Fe(μ‐SC2H4S)2Fe(NO)2]2− (3) bridged by two terminal [SC2H4S]2− ligands. On the basis of the Fe K‐edge pre‐edge energy...
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