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UV–visible absorption spectroscopy is useful for probing the electronic and structural changes of protein active sites, and thus the on‐line combination of X‐ray diffraction and spectroscopic analysis is increasingly being applied. Herein, a novel absorption spectrometer was developed at SPring‐8 BL26B2 with a nearly on‐axis geometry between the X‐ray and optical axes. A small prism mirror was placed...
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