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Stoichiometric Mo 33 Si 66 and Nb 33 Si 66 have been alloyed by mechanical alloying (MA) from the elemental powders and the process has been monitored by X-ray diffraction (XRD) technique. Nanocrystalline intermetallic compounds were obtained for either compositions: the Nb Si system gave the expected NbSi 2 compound, while in the Mo Si...
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