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A crystallochemical study was undertaken to investigate the structural stability and the compositional extent of the ternary borides M2(Ni21−xMx)B6 (M Ti, Zr, Hf). This phase often occurs during the production of MB2 joints by means of Ni–B brazing alloys. Samples with the nominal compositions M2Ni21B6 and M3Ni20B6 were synthesized by arc melting and characterized by optical and electron microscopy,...
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