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Polyphenylcarbosilane as a novel preceramic polymer for SiC was synthesized by thermal rearrangement of polymethylphenylsilane at around 350–430 °C. Characterization of the synthesized polyphenylcarbosilane was performed using 29Si NMR, 13C NMR and 1H NMR spectroscopy, FT-IR spectroscopy and TG, XRD, and GPC analysis. From the FT-IR data, the band at 1035 cm−1 was very strong and was assigned to the...
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