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The heat‐driven solid‐state transformations of K salts of the Na‐encapsulated Preyssler‐type phosphotungstates, K14[P5W30O110Na(side)(H2O)] and K14[P5W30O110Na(center)], are reported herein. K14[P5W30O110Na(side)(H2O)] contains one Na+ in one of the side cavities and a coordinating H2O molecule while K14[P5W30O110Na(center)] contains one Na+ in the central cavity. The heating of K14[P5W30O110Na(side)(H...
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