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N 1 ,N 10 -Ethyleneisoalloxazinium chloride and its 8-Cl-, 7-CF 3 -, and 3-CH 3 -7-CF 3 -substituted analogs were synthesized for the purpose of exhibiting thermal reactivity with organic substrates. The new flavins were characterized spectroscopically and electrochemically, and were found to react with amines, thiols, and phenylhydrazine, the latter case...
Two different 13 C-labeled 7-trifluoromethyl-N 1 ,N 10 -ethyleneisoalloxazinium chlorides were utilized to examine the mechanism of amine dehydrogenation. 1 H NMR studies in CD 3 CN ( 13 C NMR in DMSO-d 6 ), as confirmed using 15 N-labeled benzylamine, indicate that primary and secondary amines add to give tetrahedral...
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