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The compound 8-methoxy-5'-deoxyadenosylcobalamin (8-MeOAdoCbl), has been synthesized in 37% yield and >=95% purity by HPLC, monitored at both 254 and 525 nm, or 90+/-2% purity as judged by the 1 H NMR spectrum of the aromatic cobalamin region. This is the first synthesis of this complex in which sufficient details are reported, where a yield and purity are reported, and where key problems...
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