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The employment of alcohol-containing chelates and carboxylates in mixed Fe/Ln (Ln=lanthanide) and Fe/Y reactions has afforded a new family of [Fe III4 Ln III2 ] (Ln=Gd, Tb, Dy, Ho) and [Fe III4 Y III2 ] clusters. The reaction of [Fe 3 O(O 2 CPh) 6 (H 2 O) 3 ](NO 3 ), Ln(NO 3 ) 3 (Ln=Gd,...
The synthesis, structural characterization and magnetic properties of a new mixed ligand member of the Mn12 family are reported. The reaction of [Mn12O12(O2CPh)16(H2O)4] (4) with diphenylphosphinic acid produces [Mn12O12(O2CPh)7(O2PPh2)9)(H2O)4] (5). The crystal structure of 5 shows the [Mn12O12]16+ core is retained and exhibits two abnormally oriented Jahn-Teller elongation axes. The ligand distribution...
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