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The combined use of 1,1,1-tris(hydroxymethyl)ethane (thmeH3) and azides in Mn carboxylate chemistry has yielded a new family of decanuclear [Mn6Na4O(N3)(O2CR)5(thme)4(H2O)4] (R = Me (1); Et (2)) complexes consisting of mixed-valence Mn 2II Mn 4III units with a very rare [Mn6(μ6-O)]14+ octahedral core contained within a tetrahedron of four NaI atoms. The [Mn6Na4] units of 1 and 2 are connected via...
Three new transition metal coordination polymers based on 4,4'-bipyridine (4,4'-bipy) are reported. The reaction of 1 equiv. of nickel(II) perchlorate hexahydrate or cobalt(II) perchlorate hexahydrate with 3 equiv. of 4,4'-bipy under inert atmosphere, hydrothermal conditions yields [Ni(4,4'-bipy) 3 (H 2 O) 2 ](ClO 4 ) 2 .1.4(4,4'-bipy).3(H 2 O) (1) and...
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