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The chiral PCp-substituted phosphaferrocene 7 was prepared from the dimeric iron carbonyl complex [PCpFe(CO)2]2 (5) and t-butylphosphole (PCp=pinene-fused cyclopentadienyl). In 7, the PCp ligand is coordinated to the iron atom via its exo-side as shown by X-ray crystallography. Formylation of the sandwich complex 7 leads to a mixture of the diastereomeric aldehydes 10a,b in an approximate ratio of...
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